Synthesis, processing and testing of A poly(DL-lactide-CO-ε- caprolactone) resorbable electrospun membrane for guided tissue regeneration

P. Piyakunakorn, B. Khumraksa, B. Thapsukhon, S. Rassameemasmaung, R. Molloy, K. Suchiva, W. Punyodom

Research output: Chapter in Book/Report/Conference proceedingConference contributionpeer-review

Abstract

The aim of this study was to fabricate 75:25 poly(DL-lactide-co-ε- caprolactone), poly(DLL-co-CL) membranes for used in guided tissue regeneration (GTR). The copolymer was synthesized by ring-opening polymerization (ROP) in bulk. The 3-dimensional fiber networks with built-in microporosity membranes were prepared by electrospinning. The pore size was varied between 5-30 μm and the porosity of membrane was 69%. After immersing in phosphate buffered saline (PBS), the membranes were degradable with time, as indicated by molecular weight loss, mass weight loss, reduction of pH of the media and changes in the surface topography and shape of the membranes. However, the in vitro hydrolytic degradation of the membranes was too fast for use as periodontal GTR. The membranes maintained their original shape for the first 4 weeks and the porous structure disappeared within 2 weeks. Results from agar diffusion test suggest the membranes to be non-cytotoxic. In conclusion, the electrospun membrane was non-cytotoxic but the degradation rate was too fast to be used as GTR membrane in periodontal treatment.

Original languageEnglish
Title of host publicationBiomaterials and Applications
Pages110-113
Number of pages4
DOIs
Publication statusPublished - 2012
EventChiang Mai International Conference on Biomaterials and Applications, CMICBA 2011 - Chiang Mai, Thailand
Duration: 9 Aug 201110 Aug 2011

Publication series

NameAdvanced Materials Research
Volume506
ISSN (Print)1022-6680

Conference

ConferenceChiang Mai International Conference on Biomaterials and Applications, CMICBA 2011
Country/TerritoryThailand
CityChiang Mai
Period9/08/1110/08/11

Keywords

  • Electrospinning
  • Guided tissue regeneration
  • In vitro evaluation
  • Resorbable membrane

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